Petrochemical

Every Product On Spec. Every Certificate Auditable.

Refineries and petrochemical complexes operate under relentless process, quality, and regulatory pressure. LIMSera delivers AI-powered process intelligence, automated product certification, and custody transfer documentation — predicting quality deviations before they occur and optimising operations across every stream.

ASTM / IP Methods
Real-Time SPC
CoA Automation
ISO/IEC 17025
500+
ASTM methods pre-loaded
Real-Time
Process SPC monitoring
Auto
Certificate of Analysis
Multi-Mkt
Product spec variants

Built For Every Petrochemical Sub-Sector

Olefins & Aromatics

Ethylene, propylene, benzene, toluene, xylene purity, composition, and polymer-grade specs

Polymers & Resins

MFI, tensile, impact, DSC/TGA, additive analysis, pellet quality, co-polymer ratios

Refined Fuels

Gasoline, diesel, jet fuel, LPG — octane, cetane, sulphur, flash point, distillation

Lubricants & Base Oils

Kinematic viscosity, pour point, flash point, oxidation stability, VI, TAN/TBN

Bitumen & Asphalt

Penetration, softening point, viscosity, ductility, Marshall stability, aggregate testing

Industrial Solvents

Purity, moisture, colour, specific gravity, evaporation rate, non-volatile residue

Carbon Black

Iodine adsorption, OAN, tint strength, surface area, pellet hardness, ash content

Waxes & Paraffins

Melting point, oil content, colour, penetration, viscosity, congealing point

The Challenge

When Process Data And Lab Data Don't Talk, Off-Spec Product Reaches The Terminal.

Refineries and petrochemical complexes generate thousands of in-process and product samples every day. The analytical data from those samples must reach process engineers in minutes — not hours — to prevent off-spec production from propagating through conversion units and into finished product tanks. When laboratory and process systems are disconnected, by the time a quality deviation is identified in the LIMS, the process event that caused it has been running for half a shift.

Product certification adds another layer of complexity. A single product may carry different specification requirements for domestic markets, export customers, and blending purposes. CoAs assembled manually from multiple test sheets carry the risk of transcription errors, missing parameters, and incorrect limits being applied. Custody transfer disputes are expensive to resolve without tamper-evident, time-stamped analytical records.

LIMSera connects refinery laboratory data to process operations with AI-powered intelligence — predicting quality outcomes from in-process data, automating product certification, and maintaining ISO/IEC 17025-compliant analytical records that resolve commercial disputes and satisfy regulatory authorities worldwide.

Every Testing Domain Across Your Refinery Or Petrochemical Complex

Pre-configured for crude characterisation, process control, product release, and environmental compliance monitoring.

Crude Oil & Feedstock

Crude Oil & Feedstock

Characterise crude oil and petrochemical feedstocks with comprehensive property suites covering API gravity, viscosity, pour point, wax content, sulphur, TAN, TBN, metals by ICP-OES, distillation profiles by ASTM D86/D1160, and SARA fractionation. LIMSera manages crude assay templates that automatically generate required test lists from feedstock classification. Referee sample management ensures split samples are preserved for dispute resolution. Feedstock variability trending alerts refinery planners when incoming crude properties deviate from contracted specifications.

Key Capabilities
Crude assay template automation
API gravity, viscosity & pour point
SARA fractionation & distillation profiles
TAN, TBN & metals by ICP-OES
Feedstock variability trending alerts
Referee sample chain-of-custody

The Petrochemical Testing Workflow, End To End

01

Sample Receipt

Samples arrive from process streams, crude tankers, or finished product tanks. Barcode or QR scanning registers the sample against process unit, stream point, product lot, and collection time. Chain-of-custody is established at receipt with sample condition and seal integrity recorded.

02

Sample Preparation

Preparation instructions are loaded automatically from the method library based on sample type. Homogenisation, filtration, dilution, and conditioning steps are guided and documented. Sub-samples for multiple test streams are split and logged with full traceability to the parent container.

03

ASTM Analysis

Tests are executed following linked ASTM, IP, or EN procedures. Instrument interfaces capture raw data automatically for densitometers, viscometers, distillation units, and XRF analysers. Manual data entry is validated against method precision requirements using repeatability and reproducibility limits.

04

Specification Check

Results are automatically compared to the product specification library. Multi-market variant logic applies the correct limits based on destination. Out-of-specification results trigger immediate investigation workflows with hold on product release until resolution.

05

Technical Review

Analysts and supervisors review results with SPC trending context. Anomalous results relative to historical process performance are flagged. Instrument calibration status and reference standard validity are verified before approval. Second-person review enforced for custody transfer samples.

06

Certificate Issuance

Certificates of Analysis, quality certificates, and custody transfer certificates are auto-generated on QA approval. Digital signatures applied with QR verification. Certificates are delivered to internal planning systems, customer portals, and third-party inspection agencies simultaneously.

Quality At Every Stage

From Crude Feedstock To Certified Product

1
Feedstock
2
Cracking
3
Separation
4
Conversion
5
Blending
6
Dispatch

Everything Your Refinery Laboratory Needs

ASTM / IP Method Library

Pre-loaded ASTM, IP, EN, BIS, and ISO test method library covering 500+ petrochemical parameters. Each method defines sample type, preparation requirements, instrument type, precision statements, and specification linkage. Custom methods added without coding.

Certificate of Analysis Engine

Auto-generated CoAs with product name, lot/batch number, test results, specification limits, pass/fail status, analyst attribution, QA sign-off, and laboratory accreditation details. PDF with digital signature and QR verification code.

Statistical Process Control

Real-time SPC charting for in-process and finished product streams. Shewhart X-bar and R charts, CUSUM, EWMA, and run-rule violation detection. Process capability indices (Cp, Cpk) calculated per product parameter.

Custody Transfer Certification

Quantity and quality certificates for crude oil and product cargo movements. Tank strapping integration, temperature correction, shrinkage factor application, and multi-party sign-off workflows for commercial custody transfer documentation.

Instrument Interface Management

Direct integration with Anton Paar density meters, Grabner vapour pressure analysers, Normalab distillation units, and Spectro XRF instruments. Raw data imported automatically, outlier-flagged, and reviewed before results are committed.

Stability & Shelf-Life Tracking

Scheduled stability testing for lubricants, greases, and specialty chemicals. Pull-down alerts, result trending, and out-of-trend investigations. Accelerated stability studies with Arrhenius kinetics support for shelf-life predictions.

Turnaround Time Management

Priority-coded sample queues with TAT targets per sample type and customer. Real-time dashboards show samples approaching TAT breach. Automated escalation notifications to supervisors when targets are at risk.

Refinery Planning Integration

Laboratory results published to refinery planning and scheduling systems via API. Crude assay data feeds planning tools; in-process results update product quality prediction models in real time.

Proficiency Testing & External QC

Inter-laboratory comparison programme management including sample receipt, blind testing workflows, result submission, z-score calculation, and performance trending. ASTM Interlaboratory Study and international PT compliance tracking.

AI-Powered Quality Intelligence

Machine learning correlates feedstock composition with finished product quality, predicts specification failures from in-process data, identifies supplier variability trends, and recommends blending adjustments before off-spec product is produced. AI learns from every batch your plant processes.

Incident & OOS Investigation

Structured out-of-specification and out-of-trend investigation workflows with Phases I, II, and III analysis. AI-assisted root cause scoring, assignability determination, and formal investigation closure with regulatory documentation.

app.limsera.com — AI Process Intelligence · SPC + Prediction
2 alerts
In-process monitoring — 5 streams
Cut pointAtm. Tower
178°C
Flash pointAtm. Tower
56°C
SulphurNaphtha
42 ppmAI: trending ↑
CetaneDiesel Pool
49.8AI: predicted ↓
Smoke ptKerosene
26 mm
AI quality predictions
Diesel cetaneHigh · 91%
Will fall below 51 within 2 hoursIncrease hydrotreater severity +3°C
Naphtha sulphurMedium · 84%
Approaching 50 ppm limit by next shiftReview desulphurisation catalyst activity
AI: 2 quality risks predicted · Corrective actions recommended · Model accuracy 89%
Refinery Unit 3 · 5 streams · AI predicting · 2 corrective actions queued
AI-Powered Process Intelligence

AI That Predicts Product Quality Before The Batch Is Complete.

LIMSera's AI engine correlates in-process parameters with finished product specifications in real time. When distillation cut-point shifts at the atmospheric tower, the AI predicts the downstream impact on flash point, sulphur, and cetane number — before the product reaches the blending header. Process engineers receive actionable alerts with the predicted quality impact and recommended corrective action, not just raw data points.

SPC charts are maintained continuously with AI-powered anomaly detection that goes beyond Western Electric rules. The machine learning model identifies multi-variable correlations invisible to univariate SPC — when a combination of feed rate, temperature, and catalyst age simultaneously shifts, the AI flags the quality risk even when individual parameters remain within limits. Every prediction is logged, tracked, and correlated with actual outcomes to improve accuracy over time.

Result:Quality deviations predicted from in-process data before they reach finished product. AI-driven process optimisation that learns from every batch. Refinery-wide quality intelligence in real time.
app.limsera.com — Crude Assay & AI Feedstock Intelligence
Analysing
Cargo MV Horizon · Arab Medium · 180,000 bblVariance detected
Crude characterisation — 6 params
API Gravity31.4°32.1 ±0.8
Total Sulphur1.82%1.65 ±0.2
Vanadium42 ppm28 ±8
Nickel14 ppm11 ±4
Pour Point−12°C−15 ±3
Wax Content8.4%6.2 ±1.5
AI impact assessment
Yield predictionMedium
Diesel yield −1.8% vs plan
Catalyst impactHigh
V+Ni deposition rate ↑ — catalyst life −12%
ProcessingAction
Recommend: blend with lighter cargo in Tank 7
AI: Cargo deviation quantified · Yield impact −1.8% · Blending recommendation issued · Planner notified
MV Horizon · Arab Medium · V+Ni elevated · AI yield prediction active
Crude Assay & AI Feedstock Intelligence

AI Knows Your Crude Before It Reaches The Tower.

Every crude cargo is different. LIMSera's AI-powered crude assay module manages the complete characterisation workflow — SARA fractionation, distillation curves, metal content, sulphur speciation, and pour point profiles. The AI compares every incoming cargo against the historical assay database for that crude origin, identifying compositional shifts that would affect yield, product quality, or catalyst life.

When a cargo arrives with elevated metals, unusual viscosity, or wax content outside the historical envelope, the AI alerts planners with a quantified impact assessment — predicted yield shift, product quality change, and recommended processing adjustments — before the crude is pumped to tanks. Over time, the model builds a predictive understanding of how each crude origin behaves in your specific refinery configuration.

Result:Refinery planning decisions informed by AI-predicted yield and quality impacts. Feedstock risk identified before processing begins. Crude supplier quality trends surfaced across months and years.
app.limsera.com — Product Release & CoA Generation
Released
COA-2026-PE-0412All PASS
HDPE Film Grade · Batch B-2026-0412 · 24 tonnes
ParameterResultMethod
Density @ 15°C0.952 g/cm³D1505
Melt Flow Index1.0 g/10minD1238
Tensile Strength28.4 MPaD638
Impact Strength42 kJ/m²D256
Ash Content0.02%D5630
Certificate delivery
Customer Portal
PublishedInstant
Shipping Team
Notified< 30 sec
Inspection Agency
Delivered< 1 min
DS
Digitally signedQC Head · ISO/IEC 17025
QR verified · PDF generated · Multi-market specs applied
Batch released · CoA delivered · Dispatch cleared
HDPE Film · B-2026-0412 · 5/5 pass · CoA issued · 3 channels delivered
Product Release & Certificate Automation

CoAs That Generate Themselves. Product Release That Happens On Time.

Petrochemical product release is a race against dispatch schedules and tanker demurrage costs. LIMSera eliminates the bottleneck of manual certificate compilation. When QA approval is given, the Certificate of Analysis is generated instantly — with product name, lot number, all test results, specification limits, pass/fail status, analyst attribution, and laboratory accreditation details. Digital signatures are applied and the certificate is delivered simultaneously to the customer portal, shipping team, and third-party inspection agency.

Multi-market variant logic ensures the correct specification is applied to every CoA without manual selection. Export certificates meet destination country regulatory format requirements automatically. For aviation fuel, JIG additive treatment records and filter monitor results are included in the certificate package. Custody transfer certificates are generated with API/ASTM volume correction calculations and multi-party sign-off workflows.

Result:Product release delays eliminated. Dispatch teams receive approved CoAs before the tanker is loaded. Customer disputes answered with immutable, digitally signed analytical records.

Regulatory And Commercial Compliance Built Into Every Record.

Immutable Audit Trail

Every sample registration, result entry, OOS investigation, and approval is timestamped, user-attributed, and permanently logged. Records cannot be altered without a traceable amendment workflow.

ISO/IEC 17025 Accreditation

Proficiency testing management, measurement uncertainty recording, method validation data, and inter-laboratory comparison tracking to support ISO/IEC 17025 accreditation for petroleum testing.

OOS Investigation Framework

Three-phase out-of-specification investigation workflows with retesting authorisation, assignability determination, process review, and regulatory-compliant investigation report generation.

Environmental Permit Tracking

Regulatory permit parameter mapping, exceedance alert workflows, EPA / EU regulatory submission automation, and compliance status dashboards for refinery environmental management teams.

Auto-Generated

Product Certificate In One Click.

When a product batch passes QC review, LIMSera generates the Certificate of Analysis automatically — with test results, ASTM/IP method references, specification limits, and digital signatures. Customer-specific templates, multi-format delivery, and QR-coded verification for every certificate. ISO/IEC 17025 compliant records throughout.

ASTM/IP method refsDigital signaturesQR-verifiedISO/IEC 17025Customer templates
Certificate of AnalysisCOA-2026-PE-0412
Released
HDPE Film Grade · Batch B-2026-0412 · 24 tonnes
Melt Flow Index
1.0 g/10minD1238
Density
0.952 g/cm³D1505
Tensile Strength
28.4 MPaD638
Ash Content
0.02%D5630
DS
Digitally signedQC Head · ISO/IEC 17025
QR: Verified

Standards We Support

ISO/IEC 17025ASTM InternationalIP (Energy Institute)EN StandardsISO 9001ISO 14001ISO 45001API Q1API Q2GLP (OECD)US EPA TSCAEU REACHGHS / CLPASTM D1238 (MFI)ASTM D638 (Tensile)ASTM D1505 (Density)ASTM D86 (Distillation)ASTM D93 (Flash Point)ASTM D445 (Viscosity)ASTM D5453 (Sulphur)ASTM D4052 (Density)ASTM D6730 (PIONA)ISO 1183 (Polymer Density)ISO 527 (Plastics Tensile)EU Industrial Emissions DirectiveMARPOL Annex VI

Designed For Every Role In Your Refinery And Petrochemical Operation

Process Chemists

Real-time in-process monitoring dashboards, SPC chart access, shift handover reports, and direct linkage between laboratory results and process unit performance indicators

QC Laboratory Analysts

Guided ASTM method execution, instrument interface data capture, automatic repeatability checks, and structured OOS investigation workflows

Refinery Planners

Crude assay data feeds, product quality prediction model inputs, blending optimisation result export, and finished product quality trend dashboards

Quality Assurance Managers

Multi-level product release approval, SPC breach management, proficiency testing programme oversight, and ISO/IEC 17025 accreditation readiness dashboards

Commercial & Shipping Teams

Automated Certificate of Analysis generation, custody transfer documentation, third-party inspector portal access, and cargo quality dispute resolution records

Environmental Officers

Regulatory permit compliance per EPA, EU IED, and national agencies worldwide. Exceedance alerts, submission automation, and environmental monitoring trends

Frequently Asked Questions

Ready To Modernise Your Refinery Laboratory?

See LIMSera configured for your refinery streams, product mix, and regulatory compliance requirements.

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